Structural characterization of Chloride Salt of conducting polyaniline obtained by XRD, SAXD, SAXS and SEM E.A. Sanches a , J.C. Soares a , A.C. Mafud a,⇑ , E.G.R. Fernandes a , F.L. Leite a,b , Y.P. Mascarenhas a a University of São Paulo (USP), Institute...
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Structural characterization of Chloride Salt of conducting polyaniline obtained by XRD, SAXD, SAXS and SEM E.A. Sanches a , J.C. Soares a , A.C. Mafud a,⇑ , E.G.R. Fernandes a , F.L. Leite a,b , Y.P. Mascarenhas a a University of São Paulo (USP), Institute of Physics of São Carlos (IFSC), São Carlos, SP, Brazil b Federal University of São Carlos (UFSCar), Sorocaba, SP, Brazil h i g h l i g h t s " The structural study of polymers is always an important topic for research, since their properties are related to its structure. It was showed that the time synthesis does not improve the crystallinity of the polymer and the slow addition of the reagents promotes a better crystallinity. " The use of SAXD/XRD to obtain the full diffractogram for PANI is a new topic in the literature. The novelty of this study is a peak located at 2h = 6.2° and another one at 3.7°. " The use of SAXS, XRD and SEM techniques to characterize polymers provide a comprehensive and systematic study on the structural a
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